Determination of the total base number (TBN) in petrochemical products by potentiometric HClO4 titration
Summary
The base numbers of three different lubricating oil samples were determined. Work was carried out using different electrode systems in different solvent mixtures (glacial acetic acid/toluene and glacial acetic acid/chlorobenzene) and with different titration modes (drift and time-controlled dynamic titrations). The results obtained displayed no significant differences in their reproducibility and were all within the tolerance limits.
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Summary
The base numbers of three different lubricating oil samples were determined. Work was carried out using different electrode systems in different solvent mixtures (glacial acetic acid/toluene and glacial acetic acid/chlorobenzene) and with different titration modes (drift and time-controlled dynamic titrations). The results obtained displayed no significant differences in their reproducibility and were all within the tolerance limits.
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